Indentation recovery in GdPO4 and observation of deformation twinning

A series of nanoindentation tests on both single and polycrystalline specimens of a monazite rare-earth 12n/1200 wella orthophosphate, GdPO4, revealed frequent observation of anomalous unloading behavior with a large degree of recovery, where previously this behavior had only been observed in xenotime-structure rare-earth orthophosphates.An indentation site in the polycrystalline sample was examined using TEM dodge warlord for sale to identify the deformation mechanism responsible for recovery.The presence of a twin along the (100) orientation, along with a series of stacking faults contained within the deformation site, provide evidence that the mechanism of recovery in GdPO4 is the collapse of deformation twins during unloading.